首页   按字顺浏览 期刊浏览 卷期浏览 A reactive coevaporation system forinsitu, epitaxial YBa2Cu3O7−xthin film deposition
A reactive coevaporation system forinsitu, epitaxial YBa2Cu3O7−xthin film deposition

 

作者: Siu‐Wai Chan,   S. M. Sampere,   L. A. Farrow,   J. B. Barner,   C. T. Rogers,   B. J. Wilkens,   E. W. Chase,  

 

期刊: Journal of Vacuum Science&Technology A: Vacuum, Surfaces, and Films  (AIP Available online 1991)
卷期: Volume 9, issue 5  

页码: 2648-2652

 

ISSN:0734-2101

 

年代: 1991

 

DOI:10.1116/1.577219

 

出版商: American Vacuum Society

 

关键词: YTTRIUM OXIDES;BARIUM OXIDES;COPPER OXIDES;VACUUM SYSTEMS;SUPERCONDUCTING FILMS;HIGH−TC SUPERCONDUCTORS;DESIGN;VAPOR PHASE EPITAXY;YBa2Cu3O7

 

数据来源: AIP

 

摘要:

A new ultrahigh vacuum system has been specially designed and built to deposit high temperature superconducting thin films over a large area with great uniformity in both thickness and composition. The sources are in close proximity and a large distance (460 mm) separates the substrate holder and the sources. We will describe the design and the capabilities of the system including the design rationale. We have preparedinsituYBa2Cu3O7−xfilms to demonstrate the feasibility of the system. As configured, the reactive coevaporation system can deposit up to 35 mm diam YBa2Cu3O7−xfilms. Evaporant uniformity is expected up to 60 mm diam with the present limit in area set by the heater size, the size of the appropriate substrates, and the difficulty in attachment of substrates to the holder with uniform thermal contact. Films are prepared by coevaporation of yttrium, barium, and copper from three different evaporation sources with the substrate holder temperature measured at 680 °C in a PO2=5×10−4Torr ambient. Because the substrate holder is 460 mm above the sources, debris from the sources cannot travel upward and stick to the film surface. Films less than 250 nm thick on (001) SrTiO3and (001) LaAlO3exhibit a sharp transition width (ΔT=0.5 K) andTc(R=0)=90 K by resistivity measurements. In addition, alternating‐current (ac) magnetic susceptibility characterization shows sharp transitions (<1 K) at a slightly lower temperature implying that the induced screening current is uniform over the area of the detection coil. These films are structurally very close to single crystals as characterized by both x‐ray diffraction and Raman scattering.

 

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