AbstractPeat deposits in a gully at the inland margin of the Firth of Tay carselands contain a transgressive wedge of estuarine sediments laid down at the culmination of the Main Postglacial Transgression. In previous work, the sequence of deposits in the gully and their age have been examined at one location. The present study both extends and evaluates that previous work, employing further field work and laboratory analyses. The detailed stratigraphy of the deposits is identified, whilst from a borehole close to the limit of the transgressive deposit, diatom analysis and geochemical analyses, involving the determination of Al, Mg, C, and δ13CPDBare outlined. Eight14C assays from peat at the transgressive and regressive contacts in four boreholes along the wedge of estuarine sediments are described. Whilst the results of diatom analysis are inconclusive, the geochemical analyses indicate that the sediment accumulated broadly continuously without major changes in the depositional environment. It is concluded that the Main Postglacial Transgression in the gully was at first rapid, then slowed and culminated between 6240 ± 80 and 6030 ± 80 (or 6170 ± 90) radiocarbon years, B.P. It is subsequently maintained that the geochemical analyses described here may be of value in determining the continuity of transgressive deposits, whilst the practice of obtaining multiple radiocarbon assays at such locations should enable assessment of age to be refined. This may in turn assist in testing the hypothesis of shoreline diachroneity in glacioisostatically affected ar