13C NMR Chemical Shift Assignments in Dibucaine and Dibucaine Hydrochloride Determined by Two-Dimensional NMR Spectroscopy
作者:
LaurineA. LaPlanche,
期刊:
Spectroscopy Letters
(Taylor Available online 1991)
卷期:
Volume 24,
issue 2
页码: 209-228
ISSN:0038-7010
年代: 1991
DOI:10.1080/00387019108020651
出版商: Taylor & Francis Group
关键词: 2D Heteronuclear shift correlation;XHCORR;COLOC;13C-1H Coupling constants;Dibucaine;Dibucaine hydrochloride
数据来源: Taylor
摘要:
13C NMR chemical shift assignments were obtained for dibucaine in CDCl3and dibucaine hydrochloride in D2O solution using one-bond and long-range two-dimensional heteronuclear correlation techniques. The13C chemical shift assignments, together with the fully coupled13C spectrum, allowed the measurement of one-bond, and long-range13C1H coupling constants.
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