Apparatus for neutron diffraction at high pressure
作者:
D. B. McWhan,
D. Bloch,
G. Parisot,
期刊:
Review of Scientific Instruments
(AIP Available online 1974)
卷期:
Volume 45,
issue 5
页码: 643-646
ISSN:0034-6748
年代: 1974
DOI:10.1063/1.1686704
出版商: AIP
数据来源: AIP
摘要:
Powder neutron diffraction data have been obtained on cesium metal above the two transitions at 42.5 and 43 kilobar using a piston cylinder apparatus. A Lucalox cylinder (high density Al2O3) (35.4 mm o.d., 6.35 mm i.d.) is radially supported by compressing two steel plates with a hydraulic ram leaving a neutron window between the plates ∼6 mm high. A 17° included angle was used between the cylinder and support plates. A tungsten carbide piston, driven by a second hydraulic ram, raised the pressure on the sample at three times the rate of increase of the support pressure.
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