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Apparatus for neutron diffraction at high pressure

 

作者: D. B. McWhan,   D. Bloch,   G. Parisot,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1974)
卷期: Volume 45, issue 5  

页码: 643-646

 

ISSN:0034-6748

 

年代: 1974

 

DOI:10.1063/1.1686704

 

出版商: AIP

 

数据来源: AIP

 

摘要:

Powder neutron diffraction data have been obtained on cesium metal above the two transitions at 42.5 and 43 kilobar using a piston cylinder apparatus. A Lucalox cylinder (high density Al2O3) (35.4 mm o.d., 6.35 mm i.d.) is radially supported by compressing two steel plates with a hydraulic ram leaving a neutron window between the plates ∼6 mm high. A 17° included angle was used between the cylinder and support plates. A tungsten carbide piston, driven by a second hydraulic ram, raised the pressure on the sample at three times the rate of increase of the support pressure.

 

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