Cathodic Stripping Voltammetric Determination of Cefaclor in Pharmaceutical Formulations
作者:
L. N. C. Rodrigues,
M. V. B. Zanoni,
A. G. Fogg,
期刊:
Analytical Letters
(Taylor Available online 1999)
卷期:
Volume 32,
issue 1
页码: 97-109
ISSN:0003-2719
年代: 1999
DOI:10.1080/00032719908542601
出版商: Taylor & Francis Group
关键词: Cefaclor;Pharmaceuticals;Stripping voltammetry;Hanging Mercury Drop
数据来源: Taylor
摘要:
A sensitive method is described for the determination of cefaclor by cathodic stripping voltammetry at the hanging mercury drop electrode. cefaclor is accumulated at the electrode surface as a mercury salt, which is reduced at −0.67 V. The optimum accumulation potential and accumulation time were +0.15 V and up to 180 s, respectively. Linear calibration graphs were obtained between 3.9 μg.L−1to 39 μg.L−1and the limit of determination was evaluated to be 1.9 μg.L−1. The method was applied successfully to the determination of cefaclor in pharmaceutical formulations.
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