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Laboratory EXAFS spectrometer with a bent crystal, a solid‐state detector, and a fast detection system

 

作者: Kazuyuki Tohji,   Yasuo Udagawa,   Tsutomu Kawasaki,   Kenji Masuda,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1983)
卷期: Volume 54, issue 11  

页码: 1482-1487

 

ISSN:0034-6748

 

年代: 1983

 

DOI:10.1063/1.1137288

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A laboratory x‐ray absorption spectrometer is described which consists of a Johansson‐cut bent crystal, a rotating anode x‐ray generator, and a fast SSD (solid‐state detector). Because the SSD can completely discriminate the undesired reflections, contamination of the harmonics is avoided while maintaining a high‐source voltage necessary for strong x‐ray flux. Fast electronics equipment is employed to keep up with high‐x‐ray intensity. It is also possible to utilize higher‐order reflections for high resolving power. The data of quality comparable to those obtained at synchrotron radiation facilities can be obtained in a comparable period of time. In addition, the determination of the absolute absorbance as defined is possible, which makes the problem of the background subtraction in EXAFS analysis easy.

 

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