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1H and13C NMR Assignments of Acridine

 

作者: S. Ramaprasad,   M. Nauman,   K. Morden,  

 

期刊: Spectroscopy Letters  （Taylor Available online 1988）
卷期: Volume 21, issue 5  

页码: 383-391

 

ISSN:0038-7010

 

年代: 1988

 

DOI:10.1080/00387018808082315

 

出版商: Taylor & Francis Group

 

关键词: Acridine;2D-Correlation spectroscopy;1D-NOE1H and13C NMR assignments;Spectral simulation;ID-Inadequate

 

数据来源: Taylor

 

摘要:

A complete set of unambiguous1H and13C NMR assignments of Acridine in CDCl3has been made using nuclear overhauser (NOE) experiments and 2D NMR techniques. The usefulness of 20 Heteronuclear technique using long range (13C−1H) couplings leading to proper assignment of the two quaternary carbons in the molecule is also highlighted. Accurate (1H−1H) coupling constants obtained after a spectral simulation are presented. Several13C−1H couplings and 1-bond13C−13C couplings are also reported.

 

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