首页   按字顺浏览 期刊浏览 卷期浏览 Relating reflection boundaries in x-ray fiber diffraction patterns to specimen morpholo...
Relating reflection boundaries in x-ray fiber diffraction patterns to specimen morphology and their use for intensity measurement

 

作者: R.P. Millane,  

 

期刊: Journal of Macromolecular Science, Part B  (Taylor Available online 1989)
卷期: Volume 28, issue 2  

页码: 149-166

 

ISSN:0022-2348

 

年代: 1989

 

DOI:10.1080/00222348908215217

 

出版商: Taylor & Francis Group

 

数据来源: Taylor

 

摘要:

A description of reflection boundaries in x-ray diffraction patterns from oriented and polycrystalline polymer specimens is developed. The description is based on mosaic parameters that characterize the disorientation and crystallite size in the specimen and is independent of the exact reflection shapes. This description is part of a previously described method for measuring integrated intensities from such diffraction patterns. The reliability of the method is assessed using both numerical simulations and measurements from an x-ray fiber diffraction pattern. A method for estimating the mosaic parameters from a diffraction pattern is also described. The relevance to diffraction patterns from non-crystalline oriented polymers is also discussed.

 

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