首页   按字顺浏览 期刊浏览 卷期浏览 A plasma arc reactor for fullerene research
A plasma arc reactor for fullerene research

 

作者: T. T. Anderson,   P. L. Dyer,   J. W. Dykes,   P. Klavins,   P. E. Anderson,   J. Z. Liu,   R. N. Shelton,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1994)
卷期: Volume 65, issue 12  

页码: 3820-3822

 

ISSN:0034-6748

 

年代: 1994

 

DOI:10.1063/1.1145171

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A modified Kra¨tschmer–Huffman reactor for the mass production of fullerenes is presented. Fullerene mass production is fundamental for the synthesis of higher and endohedral fullerenes. The reactor employs mechanisms for continuous graphite‐rod feeding andinsituslag removal. Soot collects into a Soxhlet extraction thimble which serves as a fore‐line vacuum pump filter, thereby easing fullerene separation from soot. Thermal gravimetric analysis (TGA) for yield determination is reported. This TGA method is faster and uses smaller samples than Soxhlet extraction methods which rely on aromatic solvents. Production of 10 g of soot per hour is readily achieved utilizing this reactor. Fullerene yields of 20% are attained routinely. ©1994 American Institute of Physics.

 

点击下载:  PDF (420KB)



返 回