首页   按分类浏览 期刊浏览 卷期浏览 Synthesis and polymerization of various vinyl‐type monomers containing the pyrrole ring
Synthesis and polymerization of various vinyl‐type monomers containing the pyrrole ring

 

作者: Eishun Tsuchida,   Tsugikazu Tomono,   Kenji Honda,  

 

期刊: Journal of Polymer Science: Polymer Chemistry Edition  (WILEY Available online 1973)
卷期: Volume 11, issue 4  

页码: 853-872

 

ISSN:0360-6376

 

年代: 1973

 

DOI:10.1002/pol.1973.170110412

 

出版商: John Wiley&Sons, Inc.

 

数据来源: WILEY

 

摘要:

AbstractVinyl‐type monomers containing the pyrrole ring, such as 2‐vinylpyrrole (2‐VPyrr),N‐(pyrrol‐2‐yl)methylacrylamide (PMA),N‐methyl,N‐(pyrrol‐2‐yl)methylacrylamide (MPMA), 2‐allylpyrrole (2‐AP), β‐(pyrrol‐1‐yl)ethyl vinyl ether (PEVE), 2‐diallyl‐aminomethylpyrrole (DAMP), and 3‐(2‐pyrrolylmethyleneimino)propene‐1 (PIP) were synthesized by various reactions involving characteristic properties of the pyrrole ring. Radical homopolymerizations and copolymerizations of these monomers were studied. In the homopolymerization of conjugated monomers such as 2‐VPyrr and PMA, chain transfer to the pyrrole‐containing monomer was remarkable but not degradative. The copolymerization parameters, that is, the values ofr1,r2,Q1, ande1of 2‐VPyrr, were determined to be 0.066, 0.69, 5.53, and −1.36, respectively in the copolymerization of 2‐VPyrr (M1) with MMA (M2). TheQandevalues of the monomers containing a heteroaromatic ring such as 2‐vinylpyrrole, 2‐vinylfuran, and 2‐vinylthiophene were evaluated by the molecular orbital theory. Theevalue of PMA was found to be negative (−0.64) in the copolymerization with styrene, althoughefor acrylamide derivatives is generally positive. This may be explained by the intermolecular hydrogen bonding between the carbonyl group and NH group of PMA. That is, attraction or polarization of π‐electrons in the vinyl group of PMA is weakened by such hydrogen bonding. From the results of copolymerization of 2‐AP with various comonomers, the comonomers could be classified into three categories: class a monomers, in which bothQandevalues are largely positive, can copolymerize with 2‐AP; class b monomers, having smallevalues, homopolymerize and can not copolymerize with 2‐AP; classcmonomers, in which bothQandevalues are small. TheQandevalues of the comonomer must be largely posi

 

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