Steroid Synthesis by High Pressure Diels-alder Reaction of 3-methyl-2-cyclopenten-1-one
作者:
Eszter Gacs-baitz,
Assunta Marrocchi,
Lucio Minuti,
HansW. Scheeren,
Aldo Taticchi,
期刊:
Natural Product Letters
(Taylor Available online 1994)
卷期:
Volume 5,
issue 3
页码: 165-170
ISSN:1057-5634
年代: 1994
DOI:10.1080/10575639408044053
出版商: Taylor & Francis Group
关键词: Diels-Alder reaction;high pressure;steroids;9-methyl-trans-Δ6-octalone-1;1-ethenylhydronaphthalene;NMR analysis
数据来源: Taylor
摘要:
A new regioselective and diastereoselective approach to the one-step synthesis of steroid skeleton based on high pressure Diels-Alder reaction of 3-methyl-2-cyclopenten-1-one is described. Structure analysis of the reaction products by NMR spectroscopy is presented.
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