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Stereochemical differentiation and simultaneous analysis of 3‐, 4‐, and 5‐hydroxyalkanoic acids from biopolyesters by multidimensional gas chromatography

 

作者: Astrid Kaunzinger,   Frank Podebrad,   RÜDiger Liske,   Birgit Maas,   Armin Dietrich,   Armin Mosandl,  

 

期刊: Journal of High Resolution Chromatography  （WILEY Available online 1995）
卷期: Volume 18, issue 1  

页码: 49-53

 

ISSN:0935-6304

 

年代: 1995

 

DOI:10.1002/jhrc.1240180111

 

出版商: Wiley Subscription Services, Inc., A Wiley Company

 

关键词: Bacterial chiral polyesters;Hydroxy fatty acids;Enantio‐MDGC analysis

 

数据来源: WILEY

 

摘要:

AbstractThe direct enantioselective analysis of 3‐, 4‐, and 5‐hydroxy fatty acids from biological material has been achieved by enantioselective multidimensional gas chromatography (enantio‐MDGC) with heptakis(2,3‐di‐O‐methyl‐6‐O‐tert‐butyldimethylsilyl)‐ or (2,3‐di‐O‐acetyl‐6‐O‐tert‐butyldimethylsilyl)‐β‐cyclodextrin as chiral stationary phase. All the bacteria investigated produced polyesters of ena

 

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