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An improved synthesis of labelled fatty acid carboxamides.N‐phenyl [9,10(n)‐3H] oleamide andN‐[ring‐G‐13C6] phenyloleamide as standards for spanish toxic oil syndrome studies

 

作者: Josefina Casas,   Angel Messeguer,  

 

期刊: Journal of Labelled Compounds and Radiopharmaceuticals  （WILEY Available online 1991）
卷期: Volume 29, issue 7  

页码: 847-851

 

ISSN:0362-4803

 

年代: 1991

 

DOI:10.1002/jlcr.2580290716

 

出版商: John Wiley&Sons, Ltd.

 

关键词: N‐Phenyl[9,10(n)‐3H]oleamide;N‐[ring‐G‐13C6]Phenyloleamide;Synthesis;Arnides;Spanish Toxic Oil Syndrome

 

数据来源: WILEY

 

摘要:

AbstractA one‐pot procedure for the high yield preparation of title compounds is reported. The key features involve the conversion of the fatty acid into the corresponding mixed anhydride by reaction with ethyl chloroformate, followed by reaction with aniline, using acetonitrile as solvent to ensure homogeneous reaction mixtures and keeping reaction times short to avoid the formation of undesirable side product

 

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