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Self‐Balancing Laboratory Differential Refractometer

 

作者: C. J. Penther,   G. W. Noller,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1958)
卷期: Volume 29, issue 1  

页码: 43-46

 

ISSN:0034-6748

 

年代: 1958

 

DOI:10.1063/1.1716001

 

出版商: AIP

 

数据来源: AIP

 

摘要:

This refractometer is used in conjunction with a light scattering apparatus to determine high molecular weights. The self‐balancing feature relieves the operator of the tedium of making delicate visual observations while retaining high sensitivity and accuracy. Mounted on a shop surface plate it measures 15 in. wide by 18 in. long by 7 in. high exclusive of the light source transformer. A Brown Electronik amplifier and servo motor are used to position the photocells on the light beam with a repeatability of about 30 microinches. The beam deflection is read on a counter and vernier dial. The range of the instrument is 0.0175 RI unit and the stability and accuracy are within 5×10−7RI units.Differential refractometers are also useful in following fractionation by distillation or adsorption, in determining concentrations of colorless solutes in dilute solutions and in studying sedimentation equilibrium.

 

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