Nanocalorimeter for high resolution measurements of low temperature heat capacities of thin films and single crystals
作者:
Fernando Fominaya,
Thierry Fournier,
Philippe Gandit,
Jacques Chaussy,
期刊:
Review of Scientific Instruments
(AIP Available online 1997)
卷期:
Volume 68,
issue 11
页码: 4191-4195
ISSN:0034-6748
年代: 1997
DOI:10.1063/1.1148366
出版商: AIP
数据来源: AIP
摘要:
An innovative nanocalorimeter has been developed for measuring specific heats of thin films, multilayers (typical thickness: 1000 Å) and single crystals (mass: 1 &mgr;g) in the temperature range of 1.5–20 K. The addenda of the device are as small as 3 nJ/K at 4 K (0.5 nJ/K at 1.5 K), thus samples with a heat capacity of the order of nJ/K at 4 K can be measured. Heat capacity differences as a function of temperature or an external magnetic field (5 T) were determined with a resolution of&Dgr;C/C≃10−4.This way we have seen heat capacity variations of less than a pJ/K. We present as an example measurements on very smallMn12O12acetate single crystals and a measurement of a thin superconducting Pb layer. In the latter measurement we could evidence via specific heat a finite size effect. ©1997 American Institute of Physics.
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