Semi-Automated Method for Determination of Selenium in Rocks
作者:
ChrisC. Y. Chan,
M.W. A. Baig,
期刊:
Analytical Letters
(Taylor Available online 1984)
卷期:
Volume 17,
issue 2
页码: 143-155
ISSN:0003-2719
年代: 1984
DOI:10.1080/00032718408065273
出版商: Taylor & Francis Group
关键词: Selenium;semi-automated;hydride;rocks.
数据来源: Taylor
摘要:
Automted equipment is used to generate selenium hydride from solutions of rock samples prepared by digestion with a mixture of hydrofluoric, perchloric, and nitric acids. The evolved hydride is swept by argon into an electrically heated quartz tube atomizer. The atomic absorption of Se is measured at 196.0 nm. 1, 10-phenanthroline is used to minimize interferences from copper and nickel. The practical detection limit of selenium in rock samples is 0.05 pp. Results for reference rock samples agree closely with published values.
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