Versatile heteronuclear-decoupler for use with a Varian HA-100 spectrometer
作者:
R. Burton,
L. D. Hall,
期刊:
Canadian Journal of Chemistry
(NRC Available online 1970)
卷期:
Volume 48,
issue 1
页码: 59-66
ISSN:0008-4042
年代: 1970
DOI:10.1139/v70-009
出版商: NRC Research Press
数据来源: NRC
摘要:
Specific details are given for double-tuning the Varian V-4333 probe for use in the following heteronuclear magnetic double resonance experiments: observe1H at 100 MHz; irradiate2H,19F, or31P; observe19F at 94 MHz; irradiate1H,2H, or31P. An inexpensive source of audiofrequency-noise is described which, in conjunction with the double-tuned probe and several commercially available components, constitutes the basis of a versatile heteronuclear-decoupler. Examples are given which illustrate the effectiveness of this decoupler. Double-tuning of the Varian V-4333 probe by introducing a second transmitter coil is also described.
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