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Versatile heteronuclear-decoupler for use with a Varian HA-100 spectrometer

 

作者: R. Burton,   L. D. Hall,  

 

期刊: Canadian Journal of Chemistry  (NRC Available online 1970)
卷期: Volume 48, issue 1  

页码: 59-66

 

ISSN:0008-4042

 

年代: 1970

 

DOI:10.1139/v70-009

 

出版商: NRC Research Press

 

数据来源: NRC

 

摘要:

Specific details are given for double-tuning the Varian V-4333 probe for use in the following heteronuclear magnetic double resonance experiments: observe1H at 100 MHz; irradiate2H,19F, or31P; observe19F at 94 MHz; irradiate1H,2H, or31P. An inexpensive source of audiofrequency-noise is described which, in conjunction with the double-tuned probe and several commercially available components, constitutes the basis of a versatile heteronuclear-decoupler. Examples are given which illustrate the effectiveness of this decoupler. Double-tuning of the Varian V-4333 probe by introducing a second transmitter coil is also described.

 

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