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Fused Silica Capillary GC with Boron Specific Microwave Excited Plasma Detection in Derivatization and Polymer Pyrolysis

 

作者: LouisG. Sarto,   ScottA. Estes,   PeterC. Uden,   Sidney Siggia,   RamonM. Barnes,  

 

期刊: Analytical Letters  （Taylor Available online 1981）
卷期: Volume 14, issue 3  

页码: 205-218

 

ISSN:0003-2719

 

年代: 1981

 

DOI:10.1080/00032718108081397

 

出版商: Taylor & Francis Group

 

关键词: fused silica capillary GC;microwave plasma detection;boron speciation;derivatization;pyrolysis-GC

 

数据来源: Taylor

 

摘要:

Boron specific element detection for capillary column gas chromatography is achieved by atmospheric pressure microwave induced and sustained helium plasma spectroscopic emission. A small flow of hydrogen is added to the helium to enhance general plasma characteristics for boron emission. Fused silica capillary column applications are discussed for boronate derivatives of diols and in carborane silicone polymer pyrolysis.

 

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