Micellar Electrokinetic Capillary Chromatography as an Alternative Method for the Determination of Estrogens
作者:
J.J. Berzas,
G. Castañeda,
M.J. Pinilla,
期刊:
Analytical Letters
(Taylor Available online 1999)
卷期:
Volume 32,
issue 12
页码: 2453-2469
ISSN:0003-2719
年代: 1999
DOI:10.1080/00032719908542981
出版商: Taylor & Francis Group
关键词: Ethinylestradiol;Gestodene;(-)norgestrel;β-estradiol valerate;Micellar electrokinetic chromatography (MEKC);Estrogens
数据来源: Taylor
摘要:
A micellar electrokinetic chromatographic method which permits the separation of very similar compounds such as ethinylestradiol (ETE), gestodene (GTD), (-)norgestrel (LEV) and β-estradiol valerate (EST) from synthetic mixtures is described. The study was carried out at 25°C and 20 kV, using a 15 mM borate buffer (pH 9.2), 15 mM sodium dodecylsulfate (SDS) and 26% acetonitrile-water as background electrolyte. The analysis takes about 12 minutes.
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