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Microcomputer controlled integrator for Calvet‐type twin calorimeters

 

作者: K. J. Dickens,   O. J. Kleppa,   H. Yokokawa,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1980)
卷期: Volume 51, issue 5  

页码: 675-677

 

ISSN:0034-6748

 

年代: 1980

 

DOI:10.1063/1.1136280

 

出版商: AIP

 

数据来源: AIP

 

摘要:

An improved integration method has been developed for use with Calvet‐type differential calorimeters. The new integrator is based on a voltage‐to‐frequency converter combined with a digital system interfaced to a microcomputer. The microcomputer provides programmed control of the integrator and, with little or no operator intervention, calculates the total heat effect making corrections for background and baseline drift. With this method a calorimetric precision of the order of ±0.1% has been achieved in experiments carried out at 651°C. This is about one order of magnitude of improvement over graphical methods and about a factor of 3 better than the analog integration techniques which we have used previously.

 

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