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Automated nonselective measurement ofT1&rgr;by Fourier transform NMR

 

作者: Walter J. Freeman,   Thomas K. Leipert,   David L. Dalrymple,   Joseph H. Noggle,  

 

期刊: Review of Scientific Instruments  （AIP Available online 1976）
卷期: Volume 47, issue 1  

页码: 146-148

 

ISSN:0034-6748

 

年代: 1976

 

DOI:10.1063/1.1134465

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A simple, computer automated method for measuring rotating frame relaxation times (T1&rgr;) for many line spectra on modified commercial NMR spectrometers is discussed. Sources of error and critical instrumental parameters are identified. Adjustment of the various parameters of the pulsed rf system is more critical than forT1but perhaps less so than forT2measurements.

 

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