LiF (600 and 700) and plastic detector were used for measuring fast and thermal neutrons and γ-ray doses from252Cf source in tissue equivalent phantom. Conversion factors as well as related quality factors were used for absorbed and equivalent dose calculations. Two exposure positions were used: source at 30 cm and in contact with phatnom surface. The contribution of thermal and fast neutrons in both absorbed dose and equivalent dose reaches a maximum value at 3.5 cm while the maximum for γ-ray is at 8.5 cm. The build up and attenuation in tissue and the corresponding relaxation length were evaluated.