Simultaneous Determination of 4-(Indol-3-yl)Butyric and α-Naphthalene Acetic Acids in Commercial Formulations by First-Derivative Spectrofluorimetry
作者:
J.L. VILCHEZ,
R. BLANC,
A. NAVALÓN,
期刊:
Analytical Letters
(Taylor Available online 1996)
卷期:
Volume 29,
issue 2
页码: 233-248
ISSN:0003-2719
年代: 1996
DOI:10.1080/00032719608001002
出版商: Taylor & Francis Group
关键词: 4-(Indol-3-yl)butyric acid (IBA);α-Naphthalene acetic acid (NAA);Derivative spectroscopy;Spectrofluorimetry
数据来源: Taylor
摘要:
A method for the simultaneous determination of 4-(indol-3-yl)butyric acid (IBA) and α-naphthalene acetic acid (NAA) in mixtures by first-derivative spectrofluorimetry has been developed. The method is based on their native fluorescence at an apparent pH of 8.0 in an aqueous-ethanol medium (50% v/v ethanol). IBA was measured at λem= 336 nm, and NAA at λem= 358 nm. The range of application is between 0.2 and 100.0 μgl−1for IBA and between 0.2 and 50.0 μgl−1for NAA. The accuracy and precision of the method are reported. The method was applied to the determination of IBA and NAA in synthetic mixtures and commercial formulations.
点击下载:
PDF (472KB)
返 回