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Synthesis and characterization of the double cluster complexes of [(μ‐RS)(μ‐MeAs)Fe2(CO)6]2—the crystal and molecular structure of [μ‐iPrS)(μ‐MeAs)Fe2(Co)6]2

 

作者: Li‐Cheng Song,   Qing‐Mei Hu,   Jun‐Lin He,   Ru‐Ji Wang,   Hong‐Gen Wang,  

 

期刊: Heteroatom Chemistry  （WILEY Available online 1992）
卷期: Volume 3, issue 5‐6  

页码: 465-469

 

ISSN:1042-7163

 

年代: 1992

 

DOI:10.1002/hc.520030503

 

出版商: VCH Publishers, Inc.

 

数据来源: WILEY

 

摘要:

AbstractBy the reaction of [(μ‐RS (μ‐CO)Fe2(CO)6] [Et3NH] with MeAsI2, six new double cluster complexes, [(μ‐RS) (μ‐MeAs)Fe2(CO)6]2(R = Et, Pr,iPr, Bu, C5H11, Ph), were synthesized. The structure of theiPr analog was determined by single crystal X‐ray diffraction techniques. Crystal data were as follows: monoclinic, P21/n, Z = 4, a = 14.475(4), b = 13.825(3), c = 17.225(5) Å, β = 112.44(2)°, V = 3186 Å3, R = 0.0

 

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