CRYSTALLIZATION KINETICS AND PRODUCT PURITY OF α-GLUTAMIC ACID CRYSTAL
作者:
CLIFFORDY. TAI,
WEI-LI SHEI,
期刊:
Chemical Engineering Communications
(Taylor Available online 1993)
卷期:
Volume 120,
issue 1
页码: 139-152
ISSN:0098-6445
年代: 1993
DOI:10.1080/00986449308936130
出版商: Taylor & Francis Group
关键词: Glutamic acid;Crystallization kinetics;Product purity;MSMPR crystallizer
数据来源: Taylor
摘要:
A continuous mixed-suspension mixed-product removal lpar;CMSMPR) crystallizer was used to study the crystallization kinetics and product purity of glutamic acid crystal in pure solution and impure solution with L-phenylanaline as the impurity. Under the assumption that the crystal growth rate was a function of crystal size, the population balance equation was solved to give the crystal growth and nucleation rates by use of the steady-state population density data. The crystal growth and nucleation rates were suppressed by the presence of impurity. The impurity contents in the crystal products, which were analyzed by a HPLC pre-column method, were found to be related to crystal size, supersaturation, and impurity concentration of solution
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