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Evaporation Technique for Highly Refractory Substances

 

作者: H. M. O'Bryan,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1934)
卷期: Volume 5, issue 3  

页码: 125-126

 

ISSN:0034-6748

 

年代: 1934

 

DOI:10.1063/1.1751810

 

出版商: AIP

 

数据来源: AIP

 

摘要:

Platinum, boron, molybdenum, quartz and other substances have been evaporated in vacuum from a crucible heated by bombardment with electrons at 4000 volts from a tungsten filament. A small pure graphite crucible was heated to its melting point about 3500°C by 100 milliamperes of electron current. Most elements will alloy with a tantalum or molybdenum crucible so a graphite cup is usually preferable. Low melting point substances which would easily alloy with a tungsten filament can be readily handled by this method, which has been used in the preparation of x‐ray target surfaces, small mirrors and absorbing films.

 

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