Determination of Arsenic in Organic Compounds and Other Matrices by Flame Emission Spectrometry
作者:
JohnA. Dean,
RussellE. Fues,
期刊:
Analytical Letters
(Taylor Available online 1969)
卷期:
Volume 2,
issue 2
页码: 105-110
ISSN:0003-2719
年代: 1969
DOI:10.1080/00032716908051278
出版商: Taylor & Francis Group
关键词: arsenic;organo-arsenic compounds;traces of arsenic in copper or iron;flame-emission spectrometry
数据来源: Taylor
摘要:
A direct and simple method for arsenic in organic compounds involves merely dissolution of the sample in an organic solvent, such as benzene, cyclohexane, or methyl isobutyl ketone, and direct aspiration into a fuel-rich acetylene-oxygen flame. The arsenic line at 2350 Å is used; the detection limit is 2.2 ü/ml. From iron and copper matrices arsenic is isolated by extraction from a solution 9 M in HCI and 0.25 M in KI with benzene.
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