Catalytic Determination of Vanadium in Blood and Urine
作者:
GaryD. Christian,
期刊:
Analytical Letters
(Taylor Available online 1971)
卷期:
Volume 4,
issue 4
页码: 187-196
ISSN:0003-2719
年代: 1971
DOI:10.1080/00032717108058600
出版商: Taylor & Francis Group
关键词: Vanadium;catalysis;trace;blood;urine;spectrophotometry
数据来源: Taylor
摘要:
Trace amounts of vanadium catalyze the oxidation of phenylhydrazine-p-sulfonic acid by sodium chlorate. The diazonium salt produced is coupled with 1-naphthylamine to form an azodyestuff whose absorbance is read at 530 nm. Interferences ate eliminated by separating the vanadium by solvent extraction. Physiological concentrations of vanadium are determined in 10 ml. of ashed human blood or plasma and 25 ml. of ashed human urine. Recovery studies are reported along with results for the analysis of blood and urine samples.
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