RAPID ASSAY FOR THE DETERMINATION OF ZINC BACITRACIN IN FEED BY LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY
作者:
Víctor Hormazábal,
Magne Yndestad,
期刊:
Journal of Liquid Chromatography & Related Technologies
(Taylor Available online 2000)
卷期:
Volume 23,
issue 7
页码: 1083-1088
ISSN:1082-6076
年代: 2000
DOI:10.1081/JLC-100101509
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
A simple method for the determination of zinc bacitracin in feed is presented. The samples were extracted with methanol-hydrochloric acid and 1 mL of the supernatant was evaporated to c. 50 μL. After adding water and mixing, the water layer was cleaned up using LMS solid phase extraction columns, and injected to the liquid chromatography-atmospheric pressure ionization ion spray. The lower limit of quantification was 4 mg/kg in chicken and swine feed.
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