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New Mass Spectrometer Ion Source for Solids

 

作者: B. Cˇobic´,   B. Perovic´,   D. Tosˇic´,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1965)
卷期: Volume 36, issue 12  

页码: 1844-1845

 

ISSN:0034-6748

 

年代: 1965

 

DOI:10.1063/1.1719477

 

出版商: AIP

 

数据来源: AIP

 

摘要:

An ion source with magnetron geometry for mass spectrometric analysis of low vapor pressure materials is constructed. Using the magnetron configuration of this source a new method for obtaining the ion beams of low vapor pressure elements is developed. The material to be analyzed is fixed to the hot cathode, so that the cathode can be used simultaneously as a hot support for charge material and as a source of electron emission. The vapor of the material is produced by the combined effect of filament heating of charge material and cathode sputtering by the ions of carrier gas. The method was successfully applied in obtaining ions of Cr, Fe, Ti, Ir, La, Ta, Nd2O3, Re, Ce2O3, and ZrO2. The collector ion currents range up to 10−11A. The energy spread is measured by means of both the retarding potential and the beam deflection methods. It is found that there was no difference in the energy spread of this source and a classical Nier's ion source for mass spectrometry. The advantages of the source are also described.

 

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