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Reaction of mercury salts with functional organic silicon compounds

 

作者: M.G.Voronkov,   N.F.Chernov,   A.A.Tatarinova,  

 

期刊: Bulletin of the Academy of Sciences of the USSR, Division of chemical science  (Springer Available online 2004)
卷期: Volume 26, issue 8  

页码: 1700-1703

 

ISSN:0568-5230

 

年代: 2004

 

DOI:10.1007/BF00925180

 

出版商: Springer_US-Boston

 

数据来源: Springer

 

摘要:

1.Trialkyl-substituted chloro-, bromo-, and iodosilanes easily exchange a halogen atom for a mercury-salt anion during reaction with mercury acetate, benzoate, and cyanide. The reactivity in this reaction increases in going from chlorosilanes to bromo- and iodosilanes. Trialkylfluorosilanes and also trialkylalkoxy- and trialkylacetoxysilanes and hexaalkyldisiloxanes do not react with mercury salts, even during prolonged heating (up to 8 h at temperatures up to 125°C).2.The reaction of mercury salts with hexamethyldisilazane, N-organylhexamethyldisilazanes, trimethylsilyl(diorganyl)amines, and tris(trimethylsilyl)amine proceeds under mild conditions and gives acetoxymercuramines R3-nN(HgY)n, in high yields, where R=H, alkyl, or aryl and n=1, 2, or 3

 

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