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Complete13C and1H NMR Chemical Shift Assignments of 1-Nitropyrene

 

作者: BongsupP. Cho,   RobertA. Levine,   FrederickE. Evans,  

 

期刊: Spectroscopy Letters  （Taylor Available online 1991）
卷期: Volume 24, issue 1  

页码: 1-7

 

ISSN:0038-7010

 

年代: 1991

 

DOI:10.1080/00387019108018119

 

出版商: Taylor & Francis Group

 

关键词: 1-nitropyrene;two-dimensional NMR;long-range heteronuclear chemical shift correlation;bilinear rotational decoupling

 

数据来源: Taylor

 

摘要:

Ambiguities in the13C NMR chemical shift assignments of 1-nitropyrene were resolved using direct and long-range two-dimensional heteronuclear chemical shift correlation experiments. The latter was modified with a bilinear rotational decoupling (BIRD) pulse sequence, which enabled detection of all three-bond long-range correlations.

 

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