首页   按分类浏览 期刊浏览 卷期浏览 CONTRIBUTION TO THE STRUCTURE OF DISTYRENES
CONTRIBUTION TO THE STRUCTURE OF DISTYRENES

 

作者: Léo Marion,  

 

期刊: Canadian Journal of Research  (NRC Available online 1938)
卷期: Volume 16b, issue 6  

页码: 213-217

 

ISSN:1923-4287

 

年代: 1938

 

DOI:10.1139/cjr38b-029

 

出版商: NRC Research Press

 

数据来源: NRC

 

摘要:

Dehydration of αγ-diphenylbutyl alcohol with potassium bisulphate yields 1,3-diphenyl-3-butene which can be oxidized to β-phenylpropiophenone. This 3-butene isomerizes on standing to a crystalline 1,3-diphenyl-1-butene which forms a dibromo-derivative and gives benzaldehyde and hydratropic aldehyde when ozonized. If αγ-diphenylbutyl alcohol is dehydrated with 20% sulphuric acid, it also yields 1, 3-diphenyl-3 butene, but this isomerizes to 1,3-diphenyl-2-butene from which acetophenone is obtained on oxidation.Staudinger's proof of the identity of the pyrolytic distyrene with 1,3-diphenyl-3-butene is not valid since αγ-diphenylpropane, present with the distyrene, produces β-phenylpropiophenone when oxidized.

 

点击下载:  PDF (327KB)



返 回