Fast Analysis of Anabolic Steroids in Urine Samples by Electrospray Ionization Tandem Mass Spectrometry
作者:
Yoon-Seok Chang,
Jung-Suk Jang,
BongChul Chung,
期刊:
Analytical Letters
(Taylor Available online 1996)
卷期:
Volume 29,
issue 8
页码: 1389-1397
ISSN:0003-2719
年代: 1996
DOI:10.1080/00032719608001489
出版商: Taylor & Francis Group
关键词: Anabolic Steroids;Electrospray Ionization;Tandem Mass Spectrometry
数据来源: Taylor
摘要:
Unauthorized steroids were administered to volunteers and the presence of anabolic steroids in urine samples were directly confirmed by electrospray ionization mass spectrometry without using the prerequisite steps of enzymatic hydrolysis and trimethyl-chlorosilane derivatization. Further structure determination has been conducted by collisionally induced dissociation in a triple quadrupole tandem mass spectrometer. Overall, the electrospray ionization and tandem mass spectrometry methods prove to be simple, fast and sensitive for the analysis of anabolic steroids in urine samples.
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