The heat capacity of aqueous solutions of hydrofluoric acid varying in concentration from 0.55 to 48% was determined over the temperature range 18° to 20 °C. The respective values for the specific heat varied between 0.996 and 0.718 cal. per gm. The values obtained are consistent among themselves but differ markedly from those found in the literature. The apparent molal heat capacity of the solute over this range of concentration and temperature was calculated and compared with values obtained from the data of other experimenters.