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A Cyclic Voltammetry Cell for Small Sample Volumes

 

作者: DavidJ. Miner,   WilliamP. King,   PeterT. Kissinger,  

 

期刊: Analytical Letters  （Taylor Available online 1979）
卷期: Volume 12, issue 3  

页码: 213-217

 

ISSN:0003-2719

 

年代: 1979

 

DOI:10.1080/00032717908082523

 

出版商: Taylor & Francis Group

 

关键词: electrochemistry;microcell;cyclic voltammetry;metabolites

 

数据来源: Taylor

 

摘要:

A stationary-solution voltammetry cell using a unique geometry for electrode placement is described. Semimicro working and auxiliary electrodes are contained in a small sample compartment, which is isolated from a larger reference compartment by a porous glass junction. The very simple design permits cyclic voltammetry to be conveniently performed with 25–50 μL volumes containing small amounts (typ. 5 μg) of rare synthetic or isolated metabolites.

 

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