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The Glc Separation of Indole Amines and Indole Alcohols as Heptafluorobutyryl Derivatives

 

作者: J. Vessman,   A.M. Moss,   M.G. Horning,   E.C. Horning,  

 

期刊: Analytical Letters  （Taylor Available online 1969）
卷期: Volume 2, issue 2  

页码: 81-91

 

ISSN:0003-2719

 

年代: 1969

 

DOI:10.1080/00032716908051275

 

出版商: Taylor & Francis Group

 

关键词: indole amines;indole alcohols;heptafluorobutyramides;serotonin;bufotenin;N, N-dimethyltryptamine;N, N-diethyltryptamine;5-methoxy-N;N-dimethyltryptamine;5-methoxytryptamine;N-methyltryptamine;tryptamine;tryptophol;5-methoxyltryptophol;gas chromatography;m

 

数据来源: Taylor

 

摘要:

Indole amines and indole alcohols were converted to heptafluoro-butyryl (HFB) derivatives by an acyl transfer reaction with heptafluoro-butyrylimidazole. The indole NH group as well as all amino and hydroxyl groups were acylated. The HFB derivatives have excellent gas chroma-tographic properties and can be used with either hydrogen flame or electron capture detection systems. Mass spectra of the HFB derivatives of biologic N, N-dialkyl indole amines are very characteristic; these compounds can be identified easily by GLC-MS methods.

 

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