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Synthesis of Fregenedadiol Dimethyl Ether

 

作者: J.G. Urones,   I.S. Marcos,   P. Basabe,   N.M. Garrido,   A. Jorge,   R.F. Moro,   A.M. Lithgow,  

 

期刊: Natural Product Letters  （Taylor Available online 1993）
卷期: Volume 3, issue 3  

页码: 173-176

 

ISSN:1057-5634

 

年代: 1993

 

DOI:10.1080/10575639308043858

 

出版商: Taylor & Francis Group

 

关键词: Halimium viscosum;bicyclic diterpene;rearranged labdane;fregenedadiol;aromatization;cross-coupling

 

数据来源: Taylor

 

摘要:

The dienone (3β,15-dimethoxy-5,8-labdadien-7-one), obtained from 7-labdadien-3β,15-diol, is transformed into a phenol by aromatization of ring B. By a cross-coupling reaction catalyzed by Pd(0) the phenol triflate affords fregenedadiol dimethyl ether.

 

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