Densification of Large Pores: I, Expriments
作者:
Elliott B. Slamovich,
Frederick F. Lange,
期刊:
Journal of the American Ceramic Society
(WILEY Available online 1992)
卷期:
Volume 75,
issue 9
页码: 2498-2508
ISSN:0002-7820
年代: 1992
DOI:10.1111/j.1151-2916.1992.tb05603.x
出版商: Blackwell Publishing Ltd
数据来源: WILEY
摘要:
Three different diameters (0.50, 1, and 2 μm) of monosized spherical pores were introduced, at different volume percents up to 15%, into two submicrometer commercial Zr(Y)O2powders which exhibited either sluggish (ZrO2–3 mol% Y2O3) or rapid (ZrO2–8 mol% Y2O3) grain growth kinetics. Densification and grain growth behavior was studied as a function of heat‐treatment period at 1400°C and/or 1500°C. Pores in the finer‐grain Zr(3Y)O2densified more rapidly. The grain growth kinetics of the Zr(3Y)O2material were unaffected by porosity, because the pores were always larger than the grains. Consistent with the Zener concept applied to mobile pores on grain junctions, the spherical pores influenced the grain growth kinetics of Zr(8Y)O2once the grain size was greater than the pore size. Measurements indicated that the number of pores per unit volume decreased dramatically during densification, whereas their average size remained approximatel
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