SIMULTANEOUS DETERMINATION OF ALDRIN, DIELDRIN, ENDRIN, HEPTACHLOR, AND p,p’-DDT IN MEDICINAL PLANT EXTRACTS USING A NOVEL HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD
作者:
I.D. Grice,
M. Salzmann,
I. Stiff,
L.R. Griffiths,
期刊:
Journal of Liquid Chromatography & Related Technologies
(Taylor Available online 1999)
卷期:
Volume 22,
issue 15
页码: 2337-2344
ISSN:1082-6076
年代: 1999
DOI:10.1081/JLC-100101805
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
A high performance liquid chromatographic method for the simultaneous determination of five organochlorine pesticides (aldrin, p,p’-DDT, dieldrin, endrin, and heptachlor) was developed. The method was used to determine the levels of these pesticides in medicinal plant samples. Analysis was carried out using a Merck LiChrospher 100 RP C18(5 μm) column with a gradient solvent system of acetonitrile-water and PDA UV detection (224 nm). Quantification was carried out by the external standard method. The limit of detection for the utilized method was below the local legal limits (ANZFA) for similar plant materials for all 5 pesticides excepting endrin. Medicinal plant extracts were further analyzed by conventional GC-ECD and GC-NPD means using SPE and GPC cleanup as required.
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