Improved Instrument for the Measurement of Linear Pyrolysis Rates of Solids
作者:
M. K. Barsh,
W. H. Andersen,
K. W. Bills,
G. Moe,
R. D. Schultz,
期刊:
Review of Scientific Instruments
(AIP Available online 1958)
卷期:
Volume 29,
issue 5
页码: 392-395
ISSN:0034-6748
年代: 1958
DOI:10.1063/1.1716204
出版商: AIP
数据来源: AIP
摘要:
An improved instrument has been designed and constructed for the measurement of the linear decomposition and sublimation rates of solid substances. This instrument, which is provided with automatic recording devices, eliminates many of the shortcomings of the earlier prototypes and makes possible the determination of linear rates with a precision of 1%. Important new features include (1) an integral heating element and thermocouple assembly; (2) stainless‐steel and Plexiglas construction throughout; (3) heavy, solid‐copper electrical‐conductor supports for the heating element; and (4) a precision position‐sensing potentiometer. The use of cut strands of Plexiglas 55 is recommended for periodic standardization and calibration of the instrument.
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