Design of a calorimeter capable of measuring heats of adsorption on single‐crystal surfaces
作者:
D. A. Kyser,
R. I. Masel,
期刊:
Review of Scientific Instruments
(AIP Available online 1987)
卷期:
Volume 58,
issue 11
页码: 2141-2144
ISSN:0034-6748
年代: 1987
DOI:10.1063/1.1139477
出版商: AIP
数据来源: AIP
摘要:
This paper describes the design of the first calorimeter capable of measuring heats of adsorption of gases on single‐crystal surfaces in ultrahigh vacuum. The calorimeter is of the quasi‐adiabatic type, and measures the temperature rise as gas adsorbs. The calorimeter has been used to measure the heat of adsorption of CO and C2H4on Pt(111). The calorimeter seemed to perform quite well in these experiments, and yielded results that are reasonable. Thus, it is suggested that a calorimeter would be a useful addition to a surface scientist’s arsenal.
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