ION-PAIR LIQUID CHROMATOGRAPHIC DETERMINATION OF ALBENDAZOLE IN CATTLE FEED
作者:
N.A. Botsoglou,
D.J. Fletouris,
I.E. Psomas,
期刊:
Journal of Liquid Chromatography & Related Technologies
(Taylor Available online 1999)
卷期:
Volume 22,
issue 15
页码: 2297-2305
ISSN:1082-6076
年代: 1999
DOI:10.1081/JLC-100101802
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
A liquid chromatographic method is described for the determination of albendazole in cattle feeds. Samples are extracted with acetonitrile, and the extracts, after partitioning with hexane, are analyzed by ion-pair liquid chromatography with detection at 292 nm. Albendazole is eluted from the column well resolved from its oxidation byproducts. The method shows analytical characteristics well within acceptable limits. Recovery was in the range of 98.2–100.4%, while precision, expressed as percent relative standard deviation, in the range of 1.6–3.1%. Limit of detection was estimated at 0.5 μg/g, and limit of determination at 1.0 μg/g.
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