Development of a simple electrolytic jet thinning apparatus for the preparation of thin metal foils for transmission electron microscopy
作者:
T. K. Chini,
S. R. Bhattacharyya,
D. Basu,
期刊:
Review of Scientific Instruments
(AIP Available online 1994)
卷期:
Volume 65,
issue 2
页码: 370-373
ISSN:0034-6748
年代: 1994
DOI:10.1063/1.1145141
出版商: AIP
数据来源: AIP
摘要:
A very simple and inexpensive electrolytic jet thinning apparatus for rapid thinning of metal foils for transmission electron microscopy has been described. Regarding the specimen holder assembly, either a polytetrafluoroethylene (PTFE) holder or a platinum tipped locking tweezer‐type holder, can be attached electrically and mechanically to a micromanipulator to be used in the same jet thinning apparatus. This gives a unique feature to our unit, in which the specimen remains above the electrolyte during the polishing process. Also the constructional simplicity of the unit provides easy drainage of the electrolyte for lengthy polishing and a simple way of stopping the thinning process. Transmission electron micrographs of bombarded and unbombarded specimens electrothinned in the unit are presented herein.
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