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A simple high pressure flow cell for on-line absorption, Raman, and time resolved laser induced fluorescence spectroscopy in supercritical fluids

 

作者: R. Shane Addleman,   J. Ward Hills,   Chien M. Wai,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1998)
卷期: Volume 69, issue 9  

页码: 3127-3131

 

ISSN:0034-6748

 

年代: 1998

 

DOI:10.1063/1.1149071

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A versatile spectroscopic flow cell for high pressure liquids and supercritical fluid solutions is described. The cell is capable of being coupled to either standard or fiber optic spectrometers. There are two perpendicular optical paths that are adjustable in length and aperture diameter. The cell has shown it can be used for absorption, emission, or scattering spectroscopy. The design is simple, inexpensive, serviceable, uses conventional materials, and is self aligning. With apertures of 5.7 mm the cell has been tested to pressures up to 500 atm and temperatures up to 90 °C. However, the cell would allow usage at higher temperatures and pressures if desired. ©1998 American Institute of Physics.

 

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