A simple high pressure flow cell for on-line absorption, Raman, and time resolved laser induced fluorescence spectroscopy in supercritical fluids
作者:
R. Shane Addleman,
J. Ward Hills,
Chien M. Wai,
期刊:
Review of Scientific Instruments
(AIP Available online 1998)
卷期:
Volume 69,
issue 9
页码: 3127-3131
ISSN:0034-6748
年代: 1998
DOI:10.1063/1.1149071
出版商: AIP
数据来源: AIP
摘要:
A versatile spectroscopic flow cell for high pressure liquids and supercritical fluid solutions is described. The cell is capable of being coupled to either standard or fiber optic spectrometers. There are two perpendicular optical paths that are adjustable in length and aperture diameter. The cell has shown it can be used for absorption, emission, or scattering spectroscopy. The design is simple, inexpensive, serviceable, uses conventional materials, and is self aligning. With apertures of 5.7 mm the cell has been tested to pressures up to 500 atm and temperatures up to 90 °C. However, the cell would allow usage at higher temperatures and pressures if desired. ©1998 American Institute of Physics.
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