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A Novel Method for Directly Analyzing Asparagine and Glutamine by Means of Gc-Ms. Trimethylsilyl Derivatives of Thiazolinones

 

作者: MariaA. Young,   DominicM. Desiderio,  

 

期刊: Analytical Letters  （Taylor Available online 1975）
卷期: Volume 8, issue 1  

页码: 1-10

 

ISSN:0003-2719

 

年代: 1975

 

DOI:10.1080/00032717508060355

 

出版商: Taylor & Francis Group

 

关键词: Amino acids;Asparagine;Glutamine;GC-MS;TMS;Thiazol-inone;Thiohydantoin;Peptides

 

数据来源: Taylor

 

摘要:

A novel method to analyze asparagine and glutamine amino acids is presented. TMS-methylthiazolinone derivatives are prepared and hydrolysis of amide side chains is avoided. Products were elucidated by their mass spectra.

 

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