Investigation of WO42−- 3-Hydroxyflavone Complex in Water - Ethanolic Solution
作者:
D. Malešev,
Z. Radović,
M. Jelikić-Stankov,
期刊:
Spectroscopy Letters
(Taylor Available online 1992)
卷期:
Volume 25,
issue 7
页码: 1089-1095
ISSN:0038-7010
年代: 1992
DOI:10.1080/00387019208018218
出版商: Taylor & Francis Group
关键词: Spectrophotophotometric methods;pH-metry;Sodiumtungstate;3-hydroxyflavone
数据来源: Taylor
摘要:
By the application of the spectrophotometric methods the composition of the complex and by the pH-metric method the reaction of complex formation in 70% ethanol, were determined. It was found that a complex WO3(C15H9O3)22-whose concentration stability constant β2ranged from 16.45 at pH 4.0 to 11.47 at pH 7.0, was formed. Conditions were investigated for the spectrophotometric determination of 3-hydroxyflavone by means of the reaction of complex formation. It was established that in 50% ethanol 3-hydroxyflavone can be determined with great accuracy in quantities from 0.05 to 0.30 mg/ml. All investigations were carried out at room temperature (20°C) and constant values of pH and ionic strength.
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