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Densimetry in compressed fluids by combining hydrostatic weighing and magnetic levitation

 

作者: R. Masui,   W. M. Haynes,   R. F. Chang,   H. A. Davis,   J. M. H. Levelt Sengers,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1984)
卷期: Volume 55, issue 7  

页码: 1132-1142

 

ISSN:0034-6748

 

年代: 1984

 

DOI:10.1063/1.1137906

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A magnetic suspension densimeter is described that has been built for measuring the density of compressed liquids at pressures up to 15 MPa in the temperature range 20°–200°C with an uncertainty of 0.1%. The densimeter combines the principle of magnetic levitation of a buoy with that of liquid density determination by hydrostatic weighing. To accomplish this, the support coil is suspended from an electronic balance, and the balance readings are recorded (1) with the buoy at rest, and (2) with the buoy in magnetic suspension. Details are given of the construction of the cell, coil, buoy, and thermostat. The procedure is described by which cell and buoy are aligned so that the suspended buoy does not touch the cell wall. Test data on the densities of seven different liquids were obtained at room temperature. They agree with reliable literature values to within 0.1%. In a separate experiment, the bulk thermal expansion coefficient of the buoy material was determined. This experiment and its results are also given here.

 

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