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Microstructure and Densification of Pressureless‐Sintered Al2O3/Si3N4‐Whisker Composites

 

作者: Wenjea J. Tseng,   Paul D. Funkenbusch,  

 

期刊: Journal of the American Ceramic Society  (WILEY Available online 1992)
卷期: Volume 75, issue 5  

页码: 1171-1175

 

ISSN:0002-7820

 

年代: 1992

 

DOI:10.1111/j.1151-2916.1992.tb05555.x

 

出版商: Blackwell Publishing Ltd

 

关键词: composites;alumina;silicon nitride;whiskers;sintering

 

数据来源: WILEY

 

摘要:

Composite densification was studied by performing slip casting and sintering experiments on an Al2O3matrix and Si3N4whisker system. Even though all the slip‐cast powder compacts exhibited high green densities (up to 70% of the theoretical) and narrow pore‐size distribution (pore radius around 15 to 30 nm), significant differential densification on a microscopic scale was found due to the existence of local whisker agglomeration. The inhomogeneous whisker distribution resulted in a binary mixture of large and small pores in the sintered composites, in which whisker‐associated flaws remained stable even after prolonged sintering. The sintered microstructures showed that the spatial distribution as well as the volume fraction of the Si3N4affect composite densification. Inhomogeneous whisker distribution dominated the complete densification of the compo

 

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