Crystalline Methyl β-L-Pfamnofuranqside From Fischer Glycqsidatiok of L-Rhamnose
作者:
Jan Staněk,
Jitka Moravcová,
Jiří Jarý,
期刊:
Journal of Carbohydrate Chemistry
(Taylor Available online 1985)
卷期:
Volume 4,
issue 1
页码: 79-90
ISSN:0732-8303
年代: 1985
DOI:10.1080/07328308508062950
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
Flash chromatography of the mixture obtained by reaction of L-rhamnose with methanol in the presence of cation-exchange resin, in addition to methyl α-L-rhamnofuranoside (3) and methyl rhamnopyranosides1and2gave methyl β-L-rhamnofuranoside (4) in 8% yield.13C and1H NMR spectra of3and4as well as their calculated conformation in solution are discussed.
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